HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 117844610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 12982421 | HCID 12982421 | — |
| Solvent | HCID 178435160 | HCID 178435160 | — |
| Product | HCID 117844610 | HCID 117844610 | 89% |
Reaction Steps
The 1,3-diisobutylimidazolium bromide product was dissolved in deionized water (10 mL water/1 mmol salt) in a polyethylene plastic bottle. To the solution, Bio-Rad AG 1-X8 ion-exchange resin (1.1 g resin/mmol salt) was added and the slurry-like mixture was gently stirred overnight. The exchange solution was filtered and a small aliquot of the filtrate was titrated with 0.1N HCl to indicate the exchange yielded 89% of the desired 1,3-diisobutylimidazolium hydroxide product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056779B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-16089134734441eab503522fa27d2788 |
| Source note | uspto-grants-2015_06 |