HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 1,4-diazepane-1-carboxylate → HCID 86692995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 1,4-diazepane-1-carboxylate | HCID 2756058 | — |
| Reactant | 5-(2-piperazin-1-ylethyl)-2-benzofuran-1(3H)-one hydrochloride | HCID 66646732 | — |
| Reactant | 2-(1-Oxo-1,3-dihydroisobenzofuran-5-yl)acetaldehyde | HCID 77231261 | — |
| Product | HCID 86692995 | HCID 86692995 | — |
Reaction Steps
5-[2-(1,4-Diazepan-1-yl)ethyl]-2-benzofuran-1(3H)-one hydrochloride was prepared from (1-oxo-1,3-dihydro-2-benzofuran-5-yl)acetaldehyde and tert-butyl 1,4-diazepane-1-carboxylate in an analogous fashion to that described above for the synthesis of 5-(2-piperazin-1-ylethyl)-2-benzofuran-1(3H)-one hydrochloride (Method 1, steps C and D). MS: m/z 261 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-e335a6754f514e3ea67e26a37152c117 |
| Source note | uspto-grants-2015_06 |