HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl (3-fluoro-2-nitrophenyl)acetate → HCID 86693009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl (3-fluoro-2-nitrophenyl)acetate | HCID 71627086 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86693009 | HCID 86693009 | — |
Reaction Steps
A solution of methyl (3-fluoro-2-nitrophenyl)acetate (4.5 g, 21 mmol) in 100 mL of EtOAc was added 500 mg of Pd/C. The reaction was stirred at room temperature at 1 atm of H2 for 4 hours. Filtered off the catalyst and the filtration was concentrated to get methyl (2-amino-3-fluorophenyl)acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056859B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-1ccfed9f69584f7093f500a6be18af7a |
| Source note | uspto-grants-2015_06 |