HCID 86703351, compound → HCID 86703356, compound

HRID 2173683Notes

Reaction equation

HRID 2173683 reaction equation
OC1C=CC2CCCCN3C=2C=1C(=O)CC3.C[O:18][C:19]1[CH:20]=[C:21]([N:29]([CH3:31])[CH3:30])[C:22]2[C:27]([CH:28]=1)=[CH:26][CH:25]=[CH:24][CH:23]=2>>[OH:18][C:19]1[CH:20]=[C:21]([N:29]([CH3:31])[CH3:30])[C:22]2[C:27]([CH:28]=1)=[CH:26][CH:25]=[CH:24][CH:23]=2

Participants

3

Reactant 2

HCID 86703351HCID 86703351, compoundHCID 86703355HCID 86703355, compound

Product 1

HCID 86703356HCID 86703356, compound

Procedure

The title compound was synthesized in a similar manner as 11-hydroxy-2,3,5,6,7,8-hexahydro-1H-azepino[3,2,1-ij]quinolone starting from 3-methoxy-1-(dimethylamino)naphthalene: 1H NMR (DMSO-d6) δ 9.53 (s, 1H), 7.95 (d, 1H); 7.60 (d, 1H), 7.32 (ddd, 1H), 7.21 (ddd, 1H), 6.75 (d, 1H), 6.64 (d, 1H), 2.77 (s, 6H).

Sources & evidence

ORD record
ord-b2bd41cc444643e3a2408261a9dfb0fe
Source dataset
uspto-grants-2015_06
Patent number
US09056885B2

Reaction notes

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