HCID 86701503, compound → HCID 178489076, compound

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Reaction Steps

The title compound was synthesized from a mixture of (±)-tert-butyl 4-(1-(5-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)-2,2,2-trifluoro-1-methoxyethyl)-5-methoxy-7-methyl-1H-indole-1-carboxylate and (±)-tert-butyl 4-(1-(6-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)-2,2,2-trifluoro-1-methoxyethyl)-5-methoxy-7-methyl-1H-indole-1-carboxylate using the same procedure as described in Example 24-B. 1H NMR (400 MHz, DMSO-d6) δ ppm 12.76-13.01 (m, 1H) 11.06 (br. s., 1H) 8.27 (s) 7.82-7.92 (m) 7.50-7.66 (m, 2H) 7.36 (t, J=2.78 Hz, 1H) 6.65-6.79 (m, 2H) 3.19 (s, 3H) 3.10 (s, 3H). HRMS calcd. for C21H17F3N4O2 (M+H)+ 415.1379. found 415.1376.

Provenance & Evidence