HCID 86701528, compound → HCID 178489055, compound

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The title compound was synthesized from a mixture of (±)-tert-butyl 4-((5-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(dimethylamino)methyl)-5-methoxy-7-methyl-1H-indole-1-carboxylate and (±)-tert-butyl 4-((6-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(dimethylamino)methyl)-5-methoxy-7-methyl-1H-indole-1-carboxylate as described in Example 36-E. 1H NMR (400 MHz, DMSO-d6) δ ppm 12.60 (s, 1H) 10.88 (s, 1H) 7.90 (s) 7.54-7.60 (m) 7.46 (m) 7.22 (t, J=2.78 Hz, 1H) 6.74 (s, 1H) 6.69 (dd, J=2.97, 1.96 Hz, 1H) 5.38 (s, 1H) 3.79 (s, 3H) 2.41 (d, J=0.63 Hz, 3H) 2.22 (s, 6H). MS (ESI−) m/z 358.2 (M−H).

Provenance & Evidence