HCID 86701570, compound → HCID 178494644, compound

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The title compound was synthesized from a mixture of (±)-2-((5,7-dimethyl-1-tosyl-1H-indol-4-yl)(methoxy)methyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-5-carbonitrile and (±)-2-((5,7-dimethyl-1-tosyl-1H-indol-4-yl)(methoxy)methyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-6-carbonitrile as described in Example 64-B and 64-C. 1H NMR (400 MHz, DMSO-d6) δ ppm 10.96 (s, 1H) 7.96 (s, 1H) 7.63 (d, J=8.34 Hz, 1H) 7.53 (d, J=8.34 Hz, 1H) 7.20 (t, J=2.65 Hz, 1H) 6.75 (s, 1H) 6.49 (br.s, 1H) 6.21 (s, 1H) 3.35 (s, 3H) 2.43 (s, 3H) 2.42 (s, 3H). HRMS calcd. for C20H18N4O (M+H)+ 331.1553. found 331.1559.

Provenance & Evidence