HCID 86701577, compound → HCID 178424032, compound

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The title compound was synthesized from a mixture of (±)-2-(1-(5,7-dimethyl-1-tosyl-1H-indol-4-yl)ethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-5-carbonitrile and (±)-2-(1-(5,7-dimethyl-1-tosyl-1H-indol-4-yl)ethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-6-carbonitrile as described in Example 64-B and 64-C. 1H NMR (400 MHz, DMSO-d6) δ ppm 12.22 (br. s., 1H) 10.86 (br. s., 1H) 8.13 (m) 7.69-7.84 (m) 7.36-7.54 (m) 7.05 (t, J=2.78 Hz, 1H) 6.76 (s, 1H) 5.83-5.96 (m, 1H) 4.72-4.90 (m, 1H) 2.39 (s, 3H) 2.37 (s, 3H) 1.76 (d, J=7.07 Hz, 3H). HRMS calcd. for C20H18N4 (M+H)+ 315.1610. found 315.1610.

Provenance & Evidence