HCID 86701580, compound → HCID 178424034, compound

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Reaction Steps

The title compound was synthesized from a mixture of (±)-2-(1-(5,7-dimethyl-1-tosyl-1H-indol-4-yl)-1-hydroxyethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-5-carbonitrile and (±)-2-(1-(5,7-dimethyl-1-tosyl-1H-indol-4-yl)-1-hydroxyethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-6-carbonitrile following similar procedures as described in Example 64-B and 64-C. 1H NMR (400 MHz, DMSO-d6) δ ppm 12.30 (br.s, 1H) 10.80 (s, 1H) 8.18 (m) 7.77-7.82 (m) 7.48-7.54 (m) 7.07 (br. s, 1H) 6.63 (s, 1H) 6.23-6.25 (m) 5.96 (s, 1H) 2.38 (s, 3H) 2.11 (s, 3H) 2.07 (s, 3H). HRMS calcd. for C20H18N4O (M+H)+ 331.1553. found 331.1559.

Provenance & Evidence