HCID 86701605, compound → HCID 178494813, compound

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The title compound was synthesized from a mixture of (±)-2-(1-(5,7-dimethyl-1-tosyl-1H-indol-4-yl)-1-methoxyethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-5-carbonitrile and (±)-2-(1-(5,7-dimethyl-1-tosyl-1H-indol-4-yl)-1-methoxyethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-6-carbonitrile analogously to Example 64-B and 64-C. 1H NMR (TFA salt, 400 MHz, DMSO-d6) δ ppm 10.89 (s, 1H) 8.07 (s, 1H) 7.55-7.64 (m, 2H) 7.12 (t, J=2.78 Hz, 1H) 6.67 (s, 1H) 6.08 (dd, J=3.03, 2.02 Hz, 1H) 3.05 (s, 3H) 2.39 (s, 3H) 2.05 (s, 3H) 2.03 (s, 3H). HRMS calcd. for C21H20N4O (M+H)+ 345.1710. found 345.1715.

Provenance & Evidence