HCID 86701627, compound → HCID 178424036, compound

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The title compound was synthesized from a mixture of (±)-N-((5-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(5,7-dimethyl-1-tosyl-1H-indol-4-yl)methyl)-2,2,2-trifluoroacetamide and (±)-N-((6-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(5,7-dimethyl-1-tosyl-1H-indol-4-yl)methyl)-2,2,2-trifluoroacetamide as described in Example 64-B and 64-C. 1H NMR (400 MHz, DMSO-d6) δ ppm. 1H NMR (400 MHz, DMSO-d6) δ ppm 10.88 (s, 1H) 7.93 (s, 1H) 7.59 (d, J=8.08 Hz, 1H) 7.48 (app dd, J=8.34, 1.26 Hz, 1H) 7.11 (t, J=2.78 Hz, 1H) 6.73 (s, 1H) 6.19 (s, 1H) 5.77 (s, 1H) 2.43 (s, 3H) 2.39 (s, 3H). HRMS calcd. for C19H17N5 (M+H)+ 316.1557. found 316.1563.

Provenance & Evidence