HCID 86701635, compound → HCID 178483015, compound

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The title compound was synthesized from a mixture of (±)-N-((5-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(5,7-dimethyl-1-tosyl-1H-indol-4-yl)methyl)-2,2,2-trifluoro-N-methylacetamide and (±)-N-((6-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(5,7-dimethyl-1-tosyl-1H-indol-4-yl)methyl)-2,2,2-trifluoro-N-methylacetamide as described in Example 64-B and 64-C. 1H NMR (TFA salt, 400 MHz, ACETONITRILE-d3) δ ppm 9.52 (br. s, 1H) 8.00 (s, 1H) 7.54-7.62 (m, 2H) 7.16 (s, 1H) 6.98 (s, 1H) 6.33 (s, 1H) 6.06 (s, 1H) 2.68 (s, 3H) 2.55 (s, 3H) 2.49 (s, 3H). HRMS calcd. for C20H19N5 (M+H)+ 330.1713. found 330.1716.

Provenance & Evidence