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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2174029Generated: October 30, 2026

HCID 86701638, compound → HCID 178424037, compound

https://huagongshe.com/reaction/2174029

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86701638HCID 86701638—
ReactantHCID 86701639HCID 86701639—
ProductHCID 178424037HCID 178424037—

Reaction Steps

The title compound was synthesized from a mixture of (±)-N-((5-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(5,7-dimethyl-1-tosyl-1H-indol-4-yl)methyl)methanesulfonamide and (±)-N-((6-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(5,7-dimethyl-1-tosyl-1H-indol-4-yl)methyl)methanesulfonamide as described in Example 64-B and 64-C. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.01 (s, 1H) 7.97 (br. s, 1H) 7.58-7.60 (m, 1H) 7.49 (m, 1H) 7.18 (t, J=2.78 Hz, 1H) 6.78 (s, 1H) 6.35-6.37 (m, 2H) 2.82 (s, 3H) 2.44 (s, 3H) 2.42 (s, 3H). HRMS calcd. for C20H19N6O2S (M+H)+ 394.1332. found 394.1332.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09056874B2
Source datasetuspto-grants-2015_06
ORD IDord-c20a7ad84871422c9673a8c74ba5f015
Source noteuspto-grants-2015_06