HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86701638, compound → HCID 178424037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86701638 | HCID 86701638 | — |
| Reactant | HCID 86701639 | HCID 86701639 | — |
| Product | HCID 178424037 | HCID 178424037 | — |
Reaction Steps
The title compound was synthesized from a mixture of (±)-N-((5-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(5,7-dimethyl-1-tosyl-1H-indol-4-yl)methyl)methanesulfonamide and (±)-N-((6-cyano-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazol-2-yl)(5,7-dimethyl-1-tosyl-1H-indol-4-yl)methyl)methanesulfonamide as described in Example 64-B and 64-C. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.01 (s, 1H) 7.97 (br. s, 1H) 7.58-7.60 (m, 1H) 7.49 (m, 1H) 7.18 (t, J=2.78 Hz, 1H) 6.78 (s, 1H) 6.35-6.37 (m, 2H) 2.82 (s, 3H) 2.44 (s, 3H) 2.42 (s, 3H). HRMS calcd. for C20H19N6O2S (M+H)+ 394.1332. found 394.1332.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09056874B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-c20a7ad84871422c9673a8c74ba5f015 |
| Source note | uspto-grants-2015_06 |