HCID 86701652, compound → HCID 178424033, compound

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The title compound was synthesized from a mixture of (±)-2-(1-(5,7-dimethyl-1-tosyl-1H-indol-4-yl)-1-(dimethylamino)ethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-5-carbonitrile and (±)-2-(1-(5,7-dimethyl-1-tosyl-1H-indol-4-yl)-1-(dimethylamino)ethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole-6-carbonitrile as described in Example 102-B and 64-C. 1H NMR (400 MHz, CD3OD) δ ppm 7.56-8.08 (br. m, 2H), 7.55 (m, J=8.15, 1.20 Hz, 1H), 7.03 (d, J=3.23 Hz, 1H) 6.72 (s, 1H) 6.28 (d, J=3.23 Hz, 1H) 2.43 (s, 3H) 2.23 (s, 3H) 2.06 (s, 3H) 2.05 (s, 3H). HRMS calcd. for C23H26N5 (M+H)+ 358.2026. found 358.2010.

Provenance & Evidence