HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18760967, compound → HCID 131732976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18760967 | HCID 18760967 | — |
| Reactant | HCID 89389202 | HCID 89389202 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 131732976 | HCID 131732976 | — |
Reaction Steps
A solution of triphenylpyrylium tetrafluoroborate, [TPP][BF4], (100 mg, 0.252 mmol), in acetonitrile (2 ml) and a solution of potassium methyltricyanoborate (36 mg, 0.252 mmol) in acetonitril (2 ml) are combined and mixed. The salt potassium tetrafluoroborate is filtered at 0° C. and all volatile components are removed under reduced pressure resulting in the solid compound 2,4,6-triphenylpyrylium methyltricyanoborate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09058935B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-3b554d052d2e44ffac3412001c045a11 |
| Source note | uspto-grants-2015_06 |