HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyperiodinane → HCID 86712404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | HCID 86712403 | HCID 86712403 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86712404 | HCID 86712404 | 57.5% |
Reaction Steps
0.07 g of 3-[3-(8-fluoro-quinolin-3-yloxy)-pyridin-2-yl]-3-methyl-butan-2-ol were dissolved in 3 ml of dichloromethane. 0.27 g of Dess-Martin reagent were added thereto at 0° C. followed by stirring for 30 minutes. Subsequently, the reaction solution was concentrated followed by purifying by silica gel column chromatography to obtain 0.04 g of 3-[3-(8-fluoro-quinolin-3-yloxy)-pyridin-2-yl]-3-methyl-butan-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09060517B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-430419813378445ca93f467ffc033c41 |
| Source note | uspto-grants-2015_06 |