HCID 178445811, compound → 4-tert-Butylcyclohexanol

HRID 2174257Notes

Reaction equation

HRID 2174257 reaction equation
[C:1]([C@@H:5]1[CH2:10][CH2:9][C@H:8]([OH:11])[CH2:7][CH2:6]1)([CH3:4])([CH3:3])[CH3:2].C([C@H]1CC[C@H](O)CC1)(C)(C)C>>[C:1]([CH:5]1[CH2:6][CH2:7][CH:8]([OH:11])[CH2:9][CH2:10]1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 178445811HCID 178445811, compoundHCID 178445812HCID 178445812, compound

Product 1

HCID 73914-tert-Butylcyclohexanol

Procedure

A commercially available mixture consisting of 28% cis-4-tert-butyl cyclohexanol and 72% trans-4-tert-butyl cyclohexanol was purified via preparative HPLC to obtain the essentially pure cis- and trans-isomers of 4-tert-butyl cyclohexanol.

Workup

  1. customwas purified via preparative HPLC

Sources & evidence

ORD record
ord-9359f8d612964b569fa78b1c54ae568f
Source dataset
uspto-grants-2015_06
Patent number
US09060943B2

Reaction notes

Loading…