HCID 52914148, compound → HCID 52914147, compound

Participants

Reaction Steps

To a solution of compound 26 (4.26 g, 7.06 mmol) in ethanol (100 mL) was added 10% Pd/C (1.28 g). The resulting mixture was stirred under H2 (g) atmosphere at room temperature for 12 hours. The reaction mixture was filtered through a celite pad and washed with ethanol (2×20 mL). The combined filtrate was evaporated in vacuo to give an oily residue which was triturated with Et2O to provide an off-white solid 27 (3.93 g, 97% yield).

Provenance & Evidence