Dichloromethane → HCID 59235383, compound

Participants

Reaction Steps

Thionyl chloride (0.1 mL) was added dropwise into a solution of (5-chloro-4-(4-ethoxybenzyl)-2-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)phenyl)methanol (100 mg, 0.13 mmol) in methylene chloride (2 mL) at 0° C., and the mixture was allowed to stir for 2 hours at RT. The reaction mixture was evaporated to dryness, and the residual oil was used for the next step without further purification.

Provenance & Evidence