Potassium Hydroxide → HCID 67110796, compound

HRID 2174426Notes

Reaction equation

HRID 2174426 reaction equation
[OH-].[K+:2].[C:3]([OH:15])(=[O:14])/[CH:4]=[CH:5]/[C:6]1[CH:13]=[CH:12][C:10]([OH:11])=[C:8](O)[CH:7]=1>>[OH:11][C:10]1[CH:8]=[CH:7][C:6]([CH:5]=[CH:4][C:3]([O-:15])=[O:14])=[CH:13][CH:12]=1.[K+:2]

Participants

3

Reactant 2

HCID 14797Potassium HydroxideHCID 689043Caffeic Acid

Product 1

HCID 67110796HCID 67110796, compound

Procedure

To 15 mL of a 0.002 mM aqueous solution of potassium hydroxide was slowly added 5 g coumaric acid 190 (30 mmol) with mixing at 60-70° C. The resulting potassium coumarate (200) was dried under vacuum at 30-40° C.

Workup

  1. additionwith mixing at 60-70° C
  2. dry with materialThe resulting potassium coumarate (200) was dried under vacuum at 30-40° C.

Sources & evidence

ORD record
ord-1d41f0d8a1a8418888275cf2436624cd
Source dataset
uspto-grants-2015_06
Patent number
US09061993B2

Reaction notes

Loading…