Mucochloric Acid → HCID 53353682, compound

Participants

Reaction Steps

t-Butyl N′-(3,3,5,5-Tetramethylcyclohexyl)hydrazine carboxylate (5.0 g, 0.0194 moles) was suspended in 6M hydrochloric acid (375 mL) and mucochloric acid (3.28 g, 0.0194 moles) was added. Heated to reflux with stirring overnight and allowed to cool. Diluted with water and filtered off the product as a grey solid. Dried in a desiccator over phosphorus pentoxide. (4.89 g, 83%). 1H NMR (300 MHz CDCl3) 7.8 (s, 1H), 5.25 (m, 1H), 1.55 (m, 4H), 1.3 (m, 1H), 1.15 (m, 1H), 1.15 (s, 6H), 0.95 (s, 6H).

Provenance & Evidence