2-Chloro-4-phenylpyrimidine → HCID 67086889, compound
Reaction equation
[CH:1]12[CH2:7][NH:6][CH:5]1[CH2:4][N:3](C1C=NC3C(=CC=CC=3)N=1)[CH2:2]2.Cl[C:19]1[N:24]=[C:23]([C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=2)[CH:22]=[CH:21][N:20]=1>>[C:25]1([C:23]2[CH:22]=[CH:21][N:20]=[C:19]([N:3]3[CH2:4][CH:5]4[CH:1]([CH2:7][NH:6]4)[CH2:2]3)[N:24]=2)[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1Participants
3
Procedure
The title compound was prepared in a manner analogous to Intermediate 8, using 2-chloro-4-phenyl pyrimidine. MS (ESI) mass calcd. for C15H16N4, 252.31; m/z found 253.2 [M+H]+.
Sources & evidence
- ORD record
- ord-92699a0d305e46dcbd005760116ae154
- Source dataset
- uspto-grants-2015_06
- Patent number
- US09062044B2
Reaction notes
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