Hydrochloric Acid → HCID 71536643, compound

Participants

Reaction Conditions

Reaction Steps

To the solution of (76.3) (30 mg, 0.072 mmol) and 2-(aminooxy)ethanol (6.06 mg, 0.079 mmol) in MeOH (3 ml) was added a drop of 2 N HCl, sealed the tube and stirred at 50° C. for overnight. The solvent was evaporated under reduced pressure to give crude desired product as orange oil which was purified by chromatography and eluent with DCM/MeOH (30:1-20:1) to obtained pure desired product as yellow solid (25 mg, 69.4%).

Provenance & Evidence