HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Bromophenyl)acetonitrile → 2-(3-(1-(4-(2,3-Dimethylphenoxy)butanoyl)-1,2,3,4-tetrahydroquinolin-5-yl)phenyl)acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Bromophenyl)acetonitrile | HCID 36023 | — |
| Reactant | Methyl 4-bromopicolinate | HCID 12828947 | — |
| Reactant | Methyl 4-(1-(4-(2,3-dimethylphenoxy)butanoyl)-1,2,3,4-tetrahydroquinolin-5-yl)picolinate | HCID 70982851 | — |
| Product | 2-(3-(1-(4-(2,3-Dimethylphenoxy)butanoyl)-1,2,3,4-tetrahydroquinolin-5-yl)phenyl)acetonitrile | HCID 70983752 | — |
Reaction Steps
The title compound was prepared using a procedure analogous to methyl 4-(1-(4-(2,3-dimethylphenoxy)butanoyl)-1,2,3,4-tetrahydroquinolin-5-yl)picolinate except that methyl 4-bromopicolinate was replace with 2-(3-bromophenyl)acetonitrile. LCMS, [M+H]+=439.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062028B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-2ba33b6596474765b2a4d5232829052c |
| Source note | uspto-grants-2015_06 |