Trimethylphosphine → HCID 58565367, compound

Participants

Reaction Steps

To a solution of 2-(1-azidoethyl)-1-(3-fluorophenyl)-1H-indole (0.14 g, 0.50 mmol) in tetrahydrofuran (3 mL) was added 1.00 M trimethylphosphine in tetrahydrofuran (0.75 mL, 0.75 mmol). The mixture was stirred at room temperature for 1 hour. The mixture was concentrated to give crude product (0.17 g), which was used directly in the next step. LCMS calculated for C16H13FN(M-NH2)+: m/z=238.1. Found: 238.1.

Provenance & Evidence