HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyperiodinane → HCID 87943812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | HCID 69670822 | HCID 69670822 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 87943812 | HCID 87943812 | — |
Reaction Steps
To a solution of (5,6-dihydroimidazo[2,1-a]isoquinolin-2-yl)-methanol (177 mg, 0.88 mmol) in DCM (10 mL) under an atmosphere of argon was added Dess-Martin periodinane (41 mg, 0.97 mmol) and the solution stirred at room temperature for 2 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062060B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-024c9844a59042b28eec397744cbead3 |
| Source note | uspto-grants-2015_06 |