Tetrahydrofuran → HCID 90332136, compound

Participants

Reaction Steps

To a stirred solution of S-5 (3.19 g, 10.5 mmol) in THF (40 mL) was added tetrabutyl ammonium fluoride solution 1M (10.5 mL, 10.5 mmol). The resulting mixture was stirred 2 hours at room temperature and concentrated. Flash column separation using a 10-100% ethyl acetate/hexane gradient gave S-6 as an oil. (1.44 g, 72%)

Provenance & Evidence