HCID 58562482, compound → HCID 58562655, compound

HRID 2175509Notes

Reaction equation

HRID 2175509 reaction equation
O1[C:5]2([CH2:10][CH2:9][CH:8]([CH:11]3[CH2:15][O:14][C:13](=[O:16])[NH:12]3)[CH2:7][CH2:6]2)[O:4]CC1>C(#N)C>[O:4]=[C:5]1[CH2:10][CH2:9][CH:8]([CH:11]2[CH2:15][O:14][C:13](=[O:16])[NH:12]2)[CH2:7][CH2:6]1

Participants

3

Reactant 1

HCID 58562482HCID 58562482, compound

Product 1

HCID 58562655HCID 58562655, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

A solution of 4-(1,4-dioxaspiro[4.5]decan-8-yl)oxazolidin-2-one (880 mg, 3.87 mmol) and acetonitrile (65 mL).), prepared in the previous step, was deprotected as described in example 1, step C to afford the product.

Workup

  1. custom), prepared in the previous step
  2. customto afford the product

Sources & evidence

ORD record
ord-f366f1d128e9462f9d0d61a824720795
Source dataset
uspto-grants-2015_06
Patent number
US09062048B2

Reaction notes

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