1,4-Dioxaspiro[4.5]decan-8-one → HCID 57803270, compound

HRID 2175520Notes

Reaction equation

HRID 2175520 reaction equation
[CH3:1][Si:2]([CH3:9])([CH3:8])[C:3]1[S:4][CH:5]=[CH:6][N:7]=1.[O:10]1[C:14]2([CH2:19][CH2:18][C:17](=[O:20])[CH2:16][CH2:15]2)[O:13][CH2:12][CH2:11]1>>[CH3:1][Si:2]([CH3:9])([CH3:8])[C:3]1[S:4][C:5]([C:17]2([OH:20])[CH2:18][CH2:19][C:14]3([O:13][CH2:12][CH2:11][O:10]3)[CH2:15][CH2:16]2)=[CH:6][N:7]=1

Participants

3

Reactant 2

HCID 5674151,4-Dioxaspiro[4.5]decan-8-oneHCID 5884532-Trimethylsilylthiazole

Product 1

HCID 57803270HCID 57803270, compound

Procedure

The title compound was prepared as white solid from 2-trimethylsilanyl-thiazole and 1,4-dioxa-spiro[4.5]decan-8-one using the similar procedure described in Step A of Example 24. ESI-MS (m/z): Calcd. For C14H23NO3SSi, 313. found: 314 (M+H).

Sources & evidence

ORD record
ord-4488460ba3cf400e910374853f714930
Source dataset
uspto-grants-2015_06
Patent number
US09062048B2

Reaction notes

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