Trimethylsilyldiazomethane → HCID 67516395, compound

Participants

Reaction Steps

A solution of 3-amino-6,7-dihydro-5H-cyclopenta[c]pyridine-7-carboxylic acid from Step F in methanol (10 mL) was treated dropwise with a solution of trimethylsilyl diazomethane in diethyl ether (2.0 M, 1.96 mL) at 0° C. After complete addition, the reaction warmed to room temperature and stirred 30 min, then was concentrated. The resulting residue was dried under high vacuum to afford the title compound LC/MS (M+1)+=193.0;

Provenance & Evidence