3-Pentanamine → HCID 90377580, compound

HRID 2175994Notes

Reaction equation

HRID 2175994 reaction equation
[C:1]([O:5][C:6](=[O:11])[NH:7][CH2:8][CH2:9]Br)([CH3:4])([CH3:3])[CH3:2].[CH3:12][CH2:13][CH:14]([NH2:17])[CH2:15][CH3:16]>C(#N)C>[C:1]([O:5][C:6](=[O:11])[NH:7][CH2:8][CH2:9][NH:17][CH:14]([CH2:15][CH3:16])[CH2:13][CH3:12])([CH3:4])([CH3:3])[CH3:2]

Participants

4

Reactant 2

HCID 120193-PentanamineHCID 4103526tert-Butyl N-(2-bromoethyl)carbamate

Product 1

HCID 90377580HCID 90377580, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

By using 1.0 g of tert-butyl(2-bromoethyl)carbamate, 2.5 mL of pentan-3-amine, and 10 mL of acetonitrile as starting materials, the reaction similar to Preparation Example 9 was performed, thereby obtaining 890 mg of tert-butyl[2-(pentan-3-ylamino)ethyl]carbamate.

Workup

  1. customthe reaction
  2. customsimilar to Preparation Example 9

Sources & evidence

ORD record
ord-ed9c65e9978d4cddb4e3496f850df9f5
Source dataset
uspto-grants-2015_06
Patent number
US09062032B2

Reaction notes

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