Triacetoxyperiodinane → HCID 90370359, compound

Participants

Reaction Steps

By using 250 mg of methyl 4-[2-(4-{[(2-{[3-(2-hydroxyethyl)benzoyl]amino}-4,5,6,7-tetrahydro-1-benzothiophen-3-yl)carbonyl]amino}phenyl)ethyl]benzoate and 450 mg of Dess-Martin Periodinane, the reaction similar to Preparation Example 2 was performed, and then the reaction similar to Preparation Example 14 was performed, thereby obtaining 260 mg of methyl 4-{2-[4-({[2-({3-[2-(pentan-3-ylamino)ethyl]benzoyl}amino)-4,5,6,7-tetrahydro-1-benzothiophen-3-yl]carbonyl}amino)phenyl]ethyl}benzoate.

Provenance & Evidence