HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 90370156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 90370114 | HCID 90370114 | — |
| Product | HCID 90370156 | HCID 90370156 | 54.2% |
Reaction Steps
By using 375 mg of 2-(trimethylsilyl)ethyl 3-{[(5-ethoxy-5-oxopentanoyl)(pyridin-3-yl)amino]methyl}benzoate and 1.0 mL of 1.0 M TBAF (THF solution), 160 mg of 3-{[(5-ethoxy-5-oxopentanoyl)(pyridin-3-yl)amino]methyl}benzoic acid was obtained by the method similar to Preparation Example 22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062032B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-2311c4de007a4c61823f4d99fc1cb7d6 |
| Source note | uspto-grants-2015_06 |