HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67516152, compound → HCID 67515072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67516152 | HCID 67516152 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67515072 | HCID 67515072 | — |
Reaction Steps
To a solution of thieno[3,2-b]thiophene-3,6-diylbis(thiophen-3-ylmethanol) in dichloromethane at 0° C. was added pyridinium chlorochromate. The mixture was allowed to warm up at room temperature and stirred for 4 hours. The mixture was then filtered through celite. The solvent was evaporated and the resulting product was purified by column chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062152B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-d225bd42d30f4ae0a7a00f2d5cf70bdd |
| Source note | uspto-grants-2015_06 |