1-(Diphenylmethylidene)-2-phenylhydrazine → HCID 86640689, compound

HRID 2176101Notes

Reaction equation

HRID 2176101 reaction equation
[C:1]1([C:7]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[N:8][NH:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH2:23][CH2:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[CH3:31]>>[C:1]1([C:7]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[N:8][N:9]([CH2:23][CH2:24][C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=2[CH3:31])[C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 684561-(Diphenylmethylidene)-2-phenylhydrazineHCID 27569661-(2-bromoethyl)-2-methylbenzene

Product 1

HCID 86640689HCID 86640689, compound

Procedure

General procedure B was used to convert 1-(diphenylmethylene)-2-phenylhydrazine (200 mg, 0.943 mmol; Example 79A) and 1-(2-bromoethyl)-2-methylbenzene (1.46 g, 7.37 mmol; Aldrich) into the title compound: MS (DCI/NH3) m/z 391 (M+H)+.

Sources & evidence

ORD record
ord-6609f4f22ea742b1ae6ac92703b1d144
Source dataset
uspto-grants-2015_06
Patent number
US09063126B2

Reaction notes

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