HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxaldehyde, 1-methyl- → HCID 58336807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxaldehyde, 1-methyl- | HCID 12962 | — |
| Reactant | HCID 58336759 | HCID 58336759 | — |
| Product | HCID 58336807 | HCID 58336807 | — |
Reaction Steps
0.57 g (2 mmol) of 6-(l-pyridin-3-yl-1H-pyrazol-4-yl)pyridine-2-carbothioamide and 2.5 ml (27 mmol) of 1-methyl-1-formylhydrazine were stirred at 145° C. for 6 h. After cooling, the mixture was purified by chromatography on silica gel (cyclohexane/acetone).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09066518B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-0d0b50e8ae384c0b9239be862af1ff92 |
| Source note | uspto-grants-2015_06 |