HRID2176739

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID85241

(2-(2-Methoxyethoxy)ethoxy)acetic acid

C7H14O5

结构：COC(=O)N1CC[C@H]2[C@@H]1CCC[C@]2(O)C#Cc1cccc(C)c1

HCID68276168

Methyl (3aS,4R,7aS)-octahydro-4-hydroxy-4-[2-(3-methylphenyl)ethynyl]-1H-indole-1-carboxylate

C19H23NO3

PRODUCTS

生成物

结构：COCCOCCOCC(=O)O[C@@]1(C#Cc2cccc(C)c2)CCC[C@@H]2[C@H]1CCN2C(=O)OC

HCID60141748

未命名化合物

PROCEDURE

实验过程

Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and [2-(2-methoxy-ethoxy)-ethoxy]-acetic acid to yield (3aR,4S,7aR)-4-{2-[2-(2-methoxy-ethoxy)-ethoxy]-acetoxy}-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester. MS [M+H] 474; RT=7.747 min; HPLC Method I