HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbenzoic acid → HCID 60142708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbenzoic acid | HCID 7418 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60142708 | HCID 60142708 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and 3-methyl-benzoic acid to yield (3aR,4S,7aR)-methyl 4-(3-methylbenzoyloxy)-4-(m-tolylethynyl)octahydro-1H-indole-1-carboxylate. MS [M+H]=296 (ester elimination ion); RT=7.376 min; LC-MS Method II
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-7818e22622e44726a4d385eab7f4c676 |
| Source note | uspto-grants-2015_06 |