HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorobenzoic acid → HCID 60142709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorobenzoic acid | HCID 5811 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60142709 | HCID 60142709 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and 3,5-dichloro-benzoic acid to yield (3aR,4S,7aR)-methyl 4-(3,5-dichlorobenzoyloxy)-4-(m-tolylethynyl)octahydro-1H-indole-1-carboxylate. MS [M+H]=296 (ester elimination ion); RT=8.825 min; LC-MS Method II
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-247747d10e6c47a3a54c88a6b6df7605 |
| Source note | uspto-grants-2015_06 |