HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethylbenzoic acid → HCID 60142839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethylbenzoic acid | HCID 10194 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60142839 | HCID 60142839 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and 2,4,6-trimethyl-benzoic acid to yield (3aR,4S,7aR)-methyl 4-(m-tolylethynyl)-4-(2,4,6-trimethylbenzoyloxy)octahydro-1H-indole-1-carboxylate. MS [M+H]=296 (ester eliminated ion); RT=4.280 min; HPLC Method III
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-6db578c9c03e4670b42aee138adc2fc2 |
| Source note | uspto-grants-2015_06 |