HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolinic acid → HCID 60142840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolinic acid | HCID 1018 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60142840 | HCID 60142840 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and pyridine-2-carboxylic acid to yield (3aR,4S,7aR)-4-(pyridine-2-carbonyloxy)-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester. MS [M+H]=296 (ester eliminated ion); RT=3.433 min; HPLC Method III
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-57e8008d892d46a595b72ad4a26bc940 |
| Source note | uspto-grants-2015_06 |