HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxy-5-oxopentanoate → HCID 60142842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxy-5-oxopentanoate | HCID 6993194 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60142842 | HCID 60142842 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and mono-methyl glutarate to yield (3aR,4S,7aR)-1-(methoxycarbonyl)-4-(m-tolylethynyl)octahydro-1H-indol-4-yl methyl glutarate. MS [M+H]=296 (ester elimination ion); RT=1.26 min; UPLC Method I
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-6ad804ddfd4c4a3aaea77c5eb0213e7b |
| Source note | uspto-grants-2015_06 |