HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylcarbamoyl)butanoic acid → HCID 60142968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylcarbamoyl)butanoic acid | HCID 21728907 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60142968 | HCID 60142968 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and 4-dimethylcarbamoyl-butyric acid to yield (3aR,4S,7aR)-methyl 4-(5-(dimethylamino)-5-oxopentanoyloxy)-4-(m-tolylethynyl)octahydro-1H-indole-1-carboxylate. MS [2M+NH4]=927; RT=1.16 min; UPLC Method I
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-cf984d9ae5cd47adae607333e99ba101 |
| Source note | uspto-grants-2015_06 |