HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylbenzoic acid → HCID 60141189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylbenzoic acid | HCID 10356 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60141189 | HCID 60141189 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and 3,5-dimethyl-benzoic acid to yield (3aR,4S,7aR)-4-(3,5-dimethyl-benzoyloxy)-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester. MS [M+H]=296 (ester elimination ion); RT=8.590 min; LC/MS Method III
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-e2cb8b95d89d42cdb25e8ec4a629ad40 |
| Source note | uspto-grants-2015_06 |