HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorophenylacetic acid → HCID 60141330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorophenylacetic acid | HCID 81058 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60141330 | HCID 60141330 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and (2,6-dichloro-phenyl)-acetic acid to yield (3aR,4S,7aR)-4-[2-(2,6-dichloro-phenyl)-acetoxy]-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester. MS [M+H]=296 (ester elimination ion); RT=9.620 min; HPLC Method I
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-089bf59a30884e81b37597075188b3f2 |
| Source note | uspto-grants-2015_06 |