HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)benzeneacetic acid → HCID 60141332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)benzeneacetic acid | HCID 67695 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60141332 | HCID 60141332 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and (3-trifluoromethyl-phenyl)-acetic acid to yield (3aR,4S,7aR)-methyl 4-(m-tolylethynyl)-4-(2-(3-(trifluoromethyl)phenyl)acetoxy)octahydro-1H-indole-1-carboxylate. MS [M+H]=296 (ester elimination ion); RT=8.365 min; LCMS Method III
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-b01c9e1628374737a45a875580e1e85e |
| Source note | uspto-grants-2015_06 |