Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 12819459 | HCID 12819459 | — |
| Product | HCID 22716506 | HCID 22716506 | 71.3% |
Reaction Steps
Methanolic ammonia (10 ml) was added to methyl 2-(thiophen-2-yl)propanoate (200 mg, 1.17 mmol) in sealed tube, the reaction mixture was heated to 70° C. for 18 h. The volatiles were evaporated and the residue was washed with n-pentane to afford 130 mg (71.3%) of 2-(thiophen-2-yl)propanamide as brown color solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09067888B2 |
|---|
| Source dataset | uspto-grants-2015_06 |
|---|
| ORD ID | ord-46043a0b1631475988903297f0417690 |
|---|
| Source note | uspto-grants-2015_06 |
|---|
