HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12727115, compound → Ethyl 3-(pyridin-3-yl)butanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12727115 | HCID 12727115 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(pyridin-3-yl)butanoate | HCID 12727116 | 100% |
Reaction Steps
Palladium on carbon (600 mg, 10 wt. %) was added to a solution of (E)-ethyl 3-(pyridin-3-yl)but-2-enoate (0.60 g, 3.14 mmol) in EtOH (10 ml) and hydrogenated under balloon pressure for 3 h. The reaction mixture was filtered through a pad of celite and washed with EtOH. The filtrate was concentrated and dried under reduced pressure to afford 0.60 g (100%) of ethyl 3-(pyridin-3-yl)butanoate as colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067888B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-7911d072edcc432d80f59234eb17ac25 |
| Source note | uspto-grants-2015_06 |