Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2176898Generated: October 31, 2026

Ammonia → HCID 50995660, compound

https://huagongshe.com/reaction/2176898

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantEthyl 3-(pyridin-3-yl)butanoateHCID 12727116—
ProductHCID 50995660HCID 5099566047%

Reaction Steps

A solution of ethyl 3-(pyridin-3-yl)butanoate (0.50 g, 2.59 mmol) in methanolic ammonia (10 ml) was heated to 100° C. in a pressure bomb overnight. The solvent was evaporated under reduced pressure, washed with n-pentane and dried under reduced pressure to afford 0.2 g (47%) of 3-(pyridin-3-yl)butanamide as pale brown solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09067888B2
Source datasetuspto-grants-2015_06
ORD IDord-678bbbe830064e44935d2ae5dca8b0d2
Source noteuspto-grants-2015_06