HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Chlorobenzenepropanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | beta-(p-Chlorophenyl)propionic acid | HCID 123137 | — |
| Product | 4-Chlorobenzenepropanoyl chloride | HCID 12206516 | 100% |
Reaction Steps
Thionyl chloride (16.31 g, 137.09 mmol) was added to 3-(4-chlorophenyl)propionic acid (3.0 g, 16.25 mmol) at room temperature. The reaction mixture was stirred for 20 hours, then concentrated to afford 3.3 g of 3-(4-chlorophenyl)propionyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067897B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-3ca7236c33b44f44b86ecc9c4037d767 |
| Source note | uspto-grants-2015_06 |